Crude Biological Extract로 부터 완전 자동으로 HPLC-SPE Coupling System 을 이용하여 분리한 후
Fraction Collector을 이용하여 96 well plate 또는 test tube에 분취 가능
1. Sepbox2D-250
Modes of operation | Medium to non-polar, Polar Setup (optional) |
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Sample size | Max. 250 mg of extract |
Pumps | 2 HPLC pumps |
Columns | 1 injection column, 1 main separation column, 3 second separation step, 18 trap columns |
Detection | UV detector, ELSD detector (optional) |
Fraction collector | Fraction collector with microtiter plates, 24 deep-well, 48 or 96 well plates |
Modes of collection | Time and peak based |
2. Sepbox2D-2000
Gradient pump | 100 ml head, 400 bar, ternary gradient |
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Water pump | 100 ml head, 400 bar |
Valves | 13 electrically actuated valves |
njection | Up to 2,000 mg of extract with injection column technique or liquid injection using a 1ml loop |
1st separation column | 1 column, 150 x 32 mm |
2nd separation columns | 6 columns, 250 x 16 mm |
Trap columns | 18 columns, 30 x 32 mm |
UV detector | 3 mm flow cell |
ELSD detector | Splitted flow for ELSD |
Fraction collector | 12 racks, 48 vials each, max. capacity 60 ml/vial,max. 576 fractions |
3. Parallel HPLC / SFC
System | 8 channel HPLC system with Flow Control unit |
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Operating mode | Up to 8 columns in parallel |
Number of solvents | Up to 24 with optional Eluent Rack |
Pump | 10 ml pump head, incl. low pressure gradient module and online-degaser |
Operating pressure | Up to 400 bar |
Flow Control | Active flow regulation in 8 channels, flow rates 0.25 to 1.5 ml per channel, automatic purge valve |
Autosampler | Screening version, parallel injection of 1 sample at a time onto 8 columns |
Columns | Up to 250 mm length, any vendor |
Column Oven | (Optional) 8 columns, ambient temperature to 70°C |
Detector | 8x Diode Array Detector, parallel detection of the entire spectrum (200 – 600 nm) |
4. The Spematrix
System | 8 channel SFC system with Flow Control unit |
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Operating mode | Up to 8 columns in parallel |
Number of solvents | Up to 18 solvents with optional Sepmatix Eluent Rack |
CO2 pump | 100 ml pump head, 400 bar |
Modifier pump | 100 ml pump head, 400 bar |
Operating pressure | Up to 300 bar, adjustable online back pressure control |
Columns | Up to 250 mm length, any vendor |
Column Oven | (Optional) 8 columns, ambient temperature to 70° C |
Detector | 8x Diode Array Detector, 8x 10 mm flowcells, pressure stable |
5. Preparative SFC5
Operating mode | 1 analytical or semi-preparative column |
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Solvents | CO2 and organic solvents |
Number of modifier solvents | 1 standard, max. 4 solvents with optional selection valve |
Total flow rate | 50 ml/min at a modifier portion of 40 % |
CO2 pump | 30 ml pump head, 400 bar |
Modifier pump | 30 ml pump head, 400 bar |
Add - on pump | 10 ml pump head, 400 bar (optional) |
Operating pressure | Up to 300 bar, back pressure regulator online adjustable |
6. Prep SFC M5
Solvents | CO2 and organic solvents |
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Number of modifier solvents | 1 standard, max. 4 with optional selection valve |
Operating pressure | Up to 300 bar, back pressure regulator online adjustable |
Autosampler | 2 standard microtiter plates or 2 deep well MTP with 24 wells 10 ml each, racks with 60 vials 1.5 ml or 24 vials 5 ml each |
UV detector | Wavelength range 190 to 500 nm |
Other detectors | DAD, ELSD or mass spectrometer optional |
7. Prep SFC 250
Operating mode | 1 semi-preparative or preparative column |
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Solvents | CO2 and organic solvents |
Number of modifier solvents | 1 standard, 4 with optional solvent selection valve |
CO2 pump | 150 ml pump head, 400 bar |
Modifier pump | 150 ml pump head, 400 bar |
Add-on pump | 30 ml pump head, 400 bar (optional) |
Operating pressure | Up to 300 bar, back pressure regulator online adjustable |
8. Prep SFC 660
Operating mode | 1 preparative column |
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Solvents | CO2 and organic solvents |
Number of modifier solvents | 3 solvents, mixable, solvent selection valves included |
Total flow rate | 667 ml/ min at a modifier portion of 40 % |
Pump 1, CO2 | 400 ml pump head, 400 bar |
Pump 2, modifier | 250 ml pump head, 400 bar |
Pump 3, modifier/ add-on | 150 ml pump head, 400 bar |
Operating pressure | Up to 300 bar, back pressure regulator online adjustable |
UV detector | Wavelength range 190 to 500 nm |